Safety Considerations and Proposed Workflow for Laboratory-Scale Chemical Synthesis by Ball Milling

نویسندگان

چکیده

Chemical reactions that take place in a ball mill and the absence of bulk reaction solvent present different safety profiles to stirred solution reactions. Herein, we describe steps researcher may better ensure they have considered some hazards measures emerge minimize risk themselves their colleagues.

برای دانلود باید عضویت طلایی داشته باشید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Ball milling in organic synthesis: solutions and challenges.

During the last decade numerous protocols have been published using the method of ball milling for synthesis all over the field of organic chemistry. However, compared to other methods leaving their marks on the road to sustainable synthesis (e.g. microwave, ultrasound, ionic liquids) chemistry in ball mills is rather underrepresented in the knowledge of organic chemists. Especially, in the las...

متن کامل

Mechanical Synthesis of Iron and Nickel Solid Solution by High Energy Ball Milling for Packaging

Mechanical alloying (MA) is a solid-state powder processing technique involving repeated cold welding and fracturing of powder particles in a high-energy ball mill. It has been used to obtain nanocrystalline binary system FeNi. Fe and Ni elemental powders have been ball milled in a planetary mill (Pulverisette5, Fritsch) for various times up to several hours. The morphology of the powders was e...

متن کامل

Mechanochemical decomposition of pentachlorophenol by ball milling.

The mechanochemical dechlorination of pentachlorophenol (PCP) was studied using CaO and SiO2 powder as additives. The effects of the milling time and additives on the dechlorination rate were investigated. The resulting product was characterized by X-ray diffraction (XRD), Fourier transform infrared spectra (FT-IR), thermogravimetric analysis (TG) and ion chromatography (IC). It is found that g...

متن کامل

Review of Micro-Particles of Hydroxyapatite Nanoparticles by Ball Milling

Hydroxyapatite (HA) is the most important bioactive ceramics because of biocompatibility and structural similarity to the mineral part of bones and teeth of broad clinical application in the field of dentistry, orthopedic and coatings are Biomaterials. The aim of this study was to construct nano-hydroxyapatite micro particles using calcite, silica and zinc oxide using ball milling, powder, thes...

متن کامل

Synthesis of Randomly Substituted Anionic Cyclodextrins in Ball Milling.

A number of influencing factors mean that the random substitution of cyclodextrins (CD) in solution is difficult to reproduce. Reaction assembly in mechanochemistry reduces the number of these factors. However, lack of water can improve the reaction outcomes by minimizing the reagent's hydrolysis. High-energy ball milling is an efficient, green and simple method for one-step reactions and usual...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

ژورنال

عنوان ژورنال: Organic Process Research & Development

سال: 2023

ISSN: ['1083-6160', '1520-586X']

DOI: https://doi.org/10.1021/acs.oprd.2c00226